This article outlines the development and examination of the properties of an asymmetrical dissimilar metal joint produced using friction welding (FW). Friction welding involving dissimilar materials, specifically a 50 mm (length) × 45 mm (width) × 20-mm (thickness) electrolytic tough pitch copper (ETP-Cu) plate and a 12.5-mm-diameter SS304L rod, was carried out. The assessment of the asymmetrically welded components encompassed ultrasonic testing, high-pressure helium gas testing, leak testing, tensile testing, scanning electron microscopy, optical microscopy, energy-dispersive X-ray spectroscopy, X-ray diffraction analysis, hardness measurements, and elemental mapping via X-ray. Significantly, there was an observed increase in tensile strength, resulting in a joint efficiency of 86.50% compared to the ETP-Cu base material, following FW between an asymmetric ETP-Cu plate and SS304L rod. The study unveiled notable variations in the microstructure near the joint interface on the ETP-Cu material side. Intermetallic compounds, such as FeCu4 and Cu9Si phases, were detected within the reaction layer at the interface between ETP-Cu and SS304L, exhibiting a variable thickness ranging from 30 to 50 μm.