Fusion Science and Technology / Volume 54 / Number 1 / July 2008 / Pages 95-98
Technical Paper / Storage / dx.doi.org/10.13182/FST08-A1773
A hybrid-heating microwave oven provides the energy to heat small 10-gram samples of spent metal tritide storage bed material to release tenaciously held decay product 3He. Complete mass balance procedures require direct measurement of added or produced gases on a tritide bed, and over 1100°C is necessary to release deep trapped 3He. The decomposition of non-radioactive CaCO3 and the quantitative measurement of CO2 within 3% of stoichiometry demonstrate the capabilities of the apparatus to capture generated (released) gases.