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Fusion Science and Technology
Latest News
Glass strategy: Hanford’s enhanced waste glass program
The mission of the Department of Energy’s Office of River Protection (ORP) is to complete the safe cleanup of waste resulting from decades of nuclear weapons development. One of the most technologically challenging responsibilities is the safe disposition of approximately 56 million gallons of radioactive waste historically stored in 177 tanks at the Hanford Site in Washington state.
ORP has a clear incentive to reduce the overall mission duration and cost. One pathway is to develop and deploy innovative technical solutions that can advance baseline flow sheets toward higher efficiency operations while reducing identified risks without compromising safety. Vitrification is the baseline process that will convert both high-level and low-level radioactive waste at Hanford into a stable glass waste form for long-term storage and disposal.
Although vitrification is a mature technology, there are key areas where technology can further reduce operational risks, advance baseline processes to maximize waste throughput, and provide the underpinning to enhance operational flexibility; all steps in reducing mission duration and cost.
C. A. Frederick, R. R. Paguio, A. Nikroo, J. H. Hund, O. Acennas, M. Thi
Fusion Science and Technology | Volume 49 | Number 4 | May 2006 | Pages 657-662
Technical Paper | Target Fabrication | doi.org/10.13182/FST06-A1182
Articles are hosted by Taylor and Francis Online.
Resorcinol Formaldehyde (R/F) foam has been used in the fabrication of direct drive shell targets for Inertial Fusion Confinement (ICF) experiments at the University of Rochester's Laboratory for Laser Energetics (LLE). Recent cryogenic experiments at LLE using R/F shells have shown the necessity of larger pore foam compared to the standard R/F formulation. In this paper, we report controlling the pore size of R/F foam with concomitant control of the gelation time, which is crucial for successful shell fabrication. The "standard" formulation, with pores of <100 nm, was modified by decreasing the base catalyst to resorcinol concentration ratio creating a large pore R/F foam (~ >0.5 m) through reaction limited aggregation. However, this formulation decreased the gelation time, which decreased the yield of shells with proper wall uniformity (~ 30%) to an unacceptable level of <1%. We developed a technique to achieve control over the gelation time, while keeping the large pore characteristics of R/F to improve shell non-uniformity and increasing the yield to an acceptable level. We also developed a new technique for large pore formation involving changes to the acid catalyst concentration. The effects of this new formulation on the wall uniformity of shells are discussed. The pore distributions obtained using these new R/F foams were characterized using a variety of techniques, including electron microscopy, nitrogen gas adsorption, visible spectroscopy, and small angle x-ray scattering and compared to the standard small pore formulation.