Cryogenic distillation experiments were performed at TSTA with H-D-T system by using a single column and a two-column cascade. In the single column experiment, fundamental engineering data such as the liquid holdup and the HETP were measured under a variety of operational conditions. The liquid holdup in the packed section was about 10∼15% of its superficial volume. The HETP values were from 4 to 6 cm, and increased slightly with the vapor velocity. The reflux ratio had no effect on the HETP under the condition that the vapor velocity was almost constant. For the two-column experiment, dynamic behavior of the cascade was observed.