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Jeff Place on INPO’s strategy for industry growth
As executive vice president for industry strategy at the Institute of Nuclear Power Operations, Jeff Place leads INPO’s industry-facing work, engaging directly with chief nuclear officers.
Edgar Berkey, George G. Sweeney, William M. Hickam
Nuclear Technology | Volume 5 | Number 5 | November 1968 | Pages 344-353
Technical Papers and Note | doi.org/10.13182/NT68-A28002
Articles are hosted by Taylor and Francis Online.
The feasibility of using spark source mass spectrography for a direct multielement analysis of solid sodium is demonstrated. Two different sparking configurations are employed, one with the capability of obtaining local analyses and the other capable of bulk analyses. Sample handling and preparation are minimal. Both argon and vacuum are used to protect the sodium prior to analysis. Liquid nitrogen cooling applied to the sodium while sparking inhibits melting and preferential volatilization. Detection limits below 100 ppb atomic are readily attained, and there is reasonable agreement with emission spectrographs results. The analysis of doped solutions further confirms the applicability of the technique.