Home / Store / Journals / Electronic Articles / Fusion Science and Technology / Volume 37 / Number 1 / Pages 24-31
Wu-Sheng Shih, R. B. Stephens, W. J. James
Fusion Science and Technology / Volume 37 / Number 1 / Pages 24-31
Format:electronic copy (download)
Composite coatings containing beryllium are prepared by plasma-enhanced chemical vapor deposition at a substrate temperature as low as 250°C in a radio-frequency-induced cylindrical plasma reactor. Diethylberyllium is used as the precursor together with hydrogen as a coreactant gas. These coatings are characterized by Auger electron spectroscopy (AES), X-ray diffraction, X-ray photoelectron spectroscopy, scanning electron microscopy, atomic force microscopy, electrical resistivity, and thermogravimetric analysis. AES indicates that the composition of the coatings reaches a steady level at a depth of 300 Å from the surface and maintains a constant composition throughout the thickness of the coatings. The characterization studies establish the dominant phase to be Be2C. The coatings are also resistant to oxidation and hydrolysis in dry/moist air unlike bulk Be2C. It is found that the coatings deposited close to the diethylberyllium inlet contain amorphous beryllium that is homogeneously dispersed in a Be2C matrix. Films of ~5-m thickness with an acceptable permeability to H2 are prepared. These coatings meet some of the major requirements of the ablator material for inertial confinement fusion target capsules.
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